bis(acetylacetonato) palladium; triethylaluminum; triphenylphosphine in toluene T=100°C; 4 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 2 p. 263 - 266
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 348 - 352
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 4 p. 660 - 663
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 915 - 918
in benzene ratio of HCONEt2/trans-Mo(N2)2(dpe)2 100/1, refluxed under nitrogen for30 min; cooling, addn. of n-hexane, filtered, washed with ether and n-hexane, dried in vac.;
参考文献
Journal of Organometallic Chemistry, , vol. 215, # 1 p. 67 - 76