zinc in 2-methoxy-ethanol; water (N2 or Ar); mixt. of Ir complex, dppa and acid-washed Zn satd. with CO and pressurized to 4 atm; stirred at 90°C for 45 min; cooled, filtered under nitrogen, concd., chromd. on Florisil with petroleum ether-CH2Cl2 (5:1); recrystd. from THF-hexane; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 602, # 1-2 p. 137 - 143
triethylsilane; 1,2,2-trichloro-1,1,2-trichloro-ethane; palladium dichloride T=60°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 554, # 2 p. 135 - 137
1,2,2-trichloro-1,1,2-trichloro-ethane; palladium dichloride T=60°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 554, # 2 p. 135 - 137
