Villotti et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4566,4568
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Hartman
Journal of the American Chemical Society, 1955 , vol. 77, p. 5151,5153
in tetrahydrofuran; toluene byproducts: LiCl, ClSiPh3; under Ar, 1 equiv. of Li-compd. in THF was added dropwise to toluene soln. of VCl4 at -78 °C, stirring at room temp. for 24 h; solvent was removed in vac., residue was taken in CH2Cl2, LiCl was sepd., solvent was removed in vac., solid was recrystd. from CH2Cl2/n-pentane, elem. anal.;
参考文献
Preuss, Fritz; Werle, Peter
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2002 , vol. 57, # 7 p. 726 - 730
