in toluene byproducts: methane; all manipulations conducted under nitrogen excluding air and water; after 24 h standing of the reaction mixt. the formed metallic-like ppt. was removed by filtration and washed with hot toluene, filtrates combined, solvent removed by rotary evapn.;; recrystn. (hot toluene), elem. anal.;;
参考文献
Evans,W.J.; Chamberlain,L.; Ulibarri,T.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6423