4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; 2: With indium(III) chloride in tetrahydrofuran; hexane T=-78 - 20°C; 3: 4-acetylphenyl triflate With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane 1 h; Heating; Further stages.;
参考文献
Organic Letters, , vol. 1, # 8 p. 1267 - 1269
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 1 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 123, # 18 p. 4155 - 4160
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; 12 h;
参考文献
Chemistry Letters, , # 12 p. 1233 - 1234
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; water T=20°C; 12 h;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2545 - 2554
反应条件
1: 1-trimethylsilyl-2-phenylacetylene With copper(l) chloride in N,N-dimethyl-formamide T=80°C; 24 h; 2: 4-acetylphenyl triflate With tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80°C; 72 h;
参考文献
Journal of Organometallic Chemistry, , vol. 620, # 1-2 p. 282 - 286
反应条件
1: Pd(PPh3)4; Et3N / dimethylformamide / 6 h / 60 °C 2: 3 percent Chromat. / CuCl; Pd(PPh3)4 / dimethylformamide / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 6 p. 1780 - 1787
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
1: 1-trimethylsilyl-2-phenylacetylene With copper(l) chloride in N,N-dimethyl-formamide T=80°C; 24 h; 2: 4-acetylphenyl triflate With tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=80°C; 72 h;
参考文献
Journal of Organometallic Chemistry, , vol. 620, # 1-2 p. 282 - 286
反应条件
1: vinyl-magnesium bromide With indium(III) chloride in tetrahydrofuran
T=-78 - 20°C;
2: 4-acetylphenyl triflate With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran
3 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
