4-乙酰苯基三氟甲烷磺酸酯合成路线 （共 140 条）
反应条件
triphenylphosphine; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=80°C; 40 h; also with NMP; Rate constant;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=65°C; 40 h; also with other reagents; Rate constantProduct distribution;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
1: cyclopropyl bromide With tert.-butyl lithium in diethyl ether; pentane T=-78 - 20°C; 2: With indium(III) chloride in tetrahydrofuran; diethyl ether; pentane T=-78 - 20°C; 3: 4-acetylphenyl triflate With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; diethyl ether; pentane 3 h; Heating; Further stages.;
参考文献
Perez, Ignacio; Sestelo, Jose Perez; Sarandeses, Luis A.
Organic Letters, 1999 , vol. 1, # 8 p. 1267 - 1269
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; 18 h;
参考文献
Gagnon, Alexandre; Duplessis, Martin; Alsabeh, Pamela; Barabe, Francis
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3604 - 3607
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Lesma, Giordano; Sacchetti, Alessandro; Silvani, Alessandra
Synthesis, 2006 , # 4 p. 594 - 596
反应条件
tetra-n-butylammonium tetrafluoroborate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrochemical reaction;
参考文献
European Journal of Organic Chemistry, , # 9 p. 1811 - 1821
反应条件
1: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 2: 67 percent / dimethylformamide / Ambient temperature; electrolysis View Scheme
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
T=100°C; Arylation; 5 h;
参考文献
Schio, Laurent; Lemoine, Guy; Klich, Michel
Synlett, 1999 , # 10 p. 1559 - 1562
反应条件
tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; 2.5 h;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Tetrahedron Letters, 1990 , vol. 31, # 19 p. 2719 - 2722
