乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
反应条件
T=100°C; Wittig olefination; 0.166667 h; Title compound not separated from byproducts.;
参考文献
Thiemann, Thies; Watanabe, Masataka; Tanaka, Yasuko; Mataka, Shuntaro
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 578 - 584
参考文献
Bowman, W. Russell; Fletcher, Anthony J.; Lovell, Peter J.; Pedersen, Jan M.
Synlett, 2004 , # 11 p. 1905 - 1908
反应条件
sodium hydroxide in dichloromethane; water Yield given. Yields of byproduct given;
参考文献
Stambouli, A.; Chastrette, F.; Amouroux, R.; Chastrette, M.; Mattioda, G.; Blanc, A.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4149 - 4152
参考文献
Yanovskaya,L.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 774 - 780
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 857 - 865
反应条件
in tetrahydrofuran T=20°C; Wittig reaction; 12 h;
参考文献
Fernandes, Rodney A; Kumar, Pradeep
Tetrahedron, 2002 , vol. 58, # 33 p. 6685 - 6690
反应条件
manganese(IV) oxide in toluene Oxidation; Wittig reaction; 24 h; Heating;
参考文献
Blackburn, Leonie; Wei, Xudong; Taylor, Richard J. K.
Chemical Communications, 1999 , # 14 p. 1337 - 1338
反应条件
in toluene Horner-Wadsworth-Emmons olefination; 4 h; RefluxInert atmosphere; optical yield given as percent de;
参考文献
Cha, Jacob Y.; Huang, Yaodong; Pettus, Thomas R. R.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 50 p. 9519 - 9521
反应条件
sodium periodate; silica gel in diethyl ether; water T=20°C; oxidative cleavage-Witting process;
参考文献
Outram, Helen S.; Raw, Steven A.; Taylor, Richard J.K.
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6185 - 6187
反应条件
manganese(IV) oxide in dichloromethane T=20°C; oxidative cleavage-Wittig process; 24 h;
参考文献
Outram, Helen S.; Raw, Steven A.; Taylor, Richard J.K.
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6185 - 6187
反应条件
in benzene 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Bestmann, Hans Juergen; Suess, Joachim
Liebigs Annalen der Chemie, 1982 , # 2 p. 363 - 365