乙氧甲酰基亚甲基三苯基膦合成路线 (共 578 条)
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Kashiwagi, Yoshitomo; Yamanaka, Hiroshi
Heterocycles, 1988 , vol. 27, # 1 p. 257 - 260
反应条件
1: With manganese(IV) oxide; benzoic acid in dichloromethane T=20°C; 72 h; 2: With lithium aluminium tetrahydride in diethyl ether T=0°C; 1 h; 3: With manganese(IV) oxide in dichloromethane T=20°C; 78 h; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 33, # 18 p. 3233 - 3241
反应条件
triethylamine in dichloromethane Inert atmosphere;
参考文献
Rout, Laxmidhar; Harned, Andrew M.
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 12926 - 12928
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 6 p. 514 - 517
反应条件
in toluene T=80°C; 4 h;
参考文献
Li, Xiao-Dong; Kang, Shuai-Tao; Li, Guo-Yu; Li, Xian; Wang, Jin-Hui
Molecules, 2011 , vol. 16, # 5 p. 3580 - 3596
反应条件
in benzene Wittig reaction; Reflux;
参考文献
Hubschwerlen, Christian
Synthesis, 1986 , # 11 p. 962 - 964
反应条件
1: 5,6-O-isopropylidene-L-gulonic acid γ-lactone With sodium periodate; sodium hydroxide in water pH=5.5; 1 h; Inert atmosphereCooling with ice; 2: ethyl (triphenylphosphoranylidene)acetate in dichloromethane; water T=20°C; 10 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Enev, Valentin S.; Felzmann, Wolfgang; Gromov, Alexey; Marchart, Stefan; Mulzer, Johann
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9651 - 9668
反应条件
in dichloromethane T=20°C; Wittig olefination; 9 h;
参考文献
Sharma; Punna, Sreenivas; Rajendra Prasad; Krishna, Palakodety Radna; Chorghade, Mukund S.; Ley, Steven V.
Tetrahedron Asymmetry, 2005 , vol. 16, # 6 p. 1113 - 1123
反应条件
sodium periodate; sodium hydrogencarbonate 1.) ethanol, RT, 2 h, 2.) ethanol, 0 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Baskaran, S.; Trivedi, Girish.K.
Journal of Chemical Research, Miniprint, 1995 , # 8 p. 1853 - 1864
反应条件
T=100°C; Wittig olefination; 0.166667 h; Title compound not separated from byproducts.;
参考文献
Thiemann, Thies; Watanabe, Masataka; Tanaka, Yasuko; Mataka, Shuntaro
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 578 - 584