乙氧甲酰基亚甲基三苯基膦合成路线 （共 578 条）
反应条件
1: in chloroform
Wittig reaction; 10 h; Reflux;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
10 h; Reflux;
参考文献
Chang, Meng-Yang; Lin, Chung-Han; Chen, Yeh-Long; Hsu, Ru-Ting; Chang, Ching-Yao
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3154 - 3158
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=230°C; 0.333333 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Wu, Jinlong; Wu, Huafeng; Wei, Shaoyong; Dai, Wei-Min
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4401 - 4404
参考文献
Ranade, A. C.; Mali, R. S.; Kurnawal, V. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 514 - 517
反应条件
N,N-diethylaniline
0.25 h; Heating;
参考文献
Harayama, Takashi; Katsuno, Keiko; Nishita, Yoshitaka; Fujii, Masako; Abe, Hitoshi; Takeuchi, Yasuo
Heterocycles, 2001 , vol. 54, # 1 p. 319 - 328
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; Wittig olefination; 24 h;
参考文献
Phillips, David J.; Pillinger, Kathryn S.; Li, Wei; Taylor, Angela E.; Graham, Andrew E.
Tetrahedron, 2007 , vol. 63, # 42 p. 10528 - 10533
参考文献
Kovalev,B.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1969 , vol. 5, p. 1722 - 1726
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 1775 - 1779
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998
反应条件
in ethylbenzene
10 h; Heating;
参考文献
Kelkar, Shriniwas L.; Phadke, Chetan P.; Marina, Sister
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 458 - 459
反应条件
pyridine in dichloromethane
3 h; Ambient temperature;
参考文献
Lee, Hyi-Seung; Kim, Kyongtae
Tetrahedron Letters, 1996 , vol. 37, # 6 p. 869 - 872
参考文献
Xie, Lan; Takeuchi, Yasuo; Cosentino, L. Mark; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 16 p. 2151 - 2156
