反应条件
n-butyllithium in tetrahydrofuran; hexane addn. and stirring BuLi in hexane and furan in anhyd. THF at -30°C under N2 (1.5 h), addn. of tributylchlorostannane, stirring at -30°C (0.5 h); addn. of satd. aq. NaHCO3, sepn. of the org. phase, washing with satd. aq. NaHCO3 and brine, drying with Na2CO3, evapn., column chromy. (neutral Al2O3, light petroleum), oily compd., elem. anal.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2415 - 2422