2,5-二甲基-2,5-己二醇合成路线 (共 107 条)
反应条件
hydrogen; 0.25 Pd/Al2O3 in xylene T=80°C; P=22502.3 Torr; Product distribution / selectivity;
参考文献
EP1161407 B1, ;
Page/Page column 14-15 ;
反应条件
sodium tetrahydroborate; Fe pythalocyanine; dimethylsulfide; oxygen in ethanol T=20°C; P=760.051 Torr;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 10 p. 2730 - 2734
Angew. Chem., , vol. 126, # 10 p. 2768 - 2772,5
反应条件
sodium tetrahydroborate; Fe pythalocyanine; dimethylsulfide; oxygen in ethanol T=20°C; P=760.051 Torr;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 10 p. 2730 - 2734
Angew. Chem., , vol. 126, # 10 p. 2768 - 2772,5
反应条件
sulfuric acid; dihydrogen peroxide; iron(II) sulfate
参考文献
Journal of the American Chemical Society, , vol. 80, p. 2864,2870
Org.Synth.Coll.Vol.V<1973>1026
反应条件
1: (i) Mg, (ii) /BRN= 635680/ 2: KMnO4 / H2O View Scheme
参考文献
Journal of the American Chemical Society, , vol. 82, p. 4249 - 4252
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1887 - 1892
反应条件
sulfuric acid; dihydrogen peroxide; iron(II) sulfate P=36775.4 Torr;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 2882,2886
反应条件
1: (i) O2, (irradiation), (ii) 4-nonyl-benzenethiol, NaOMe 2: H2 / Pd-C / methanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1887 - 1892
反应条件
dihydrogen peroxide; iron(II) chloride in water T=0 - 20°C; Dimerization; chlorination; pH=2; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 40, # 52 p. 9201 - 9204
反应条件
potassium permanganate in water
参考文献
Journal of the American Chemical Society, , vol. 82, p. 4249 - 4252