2,5-二甲基-2,5-己二醇合成路线 （共 107 条）
反应条件
1: hydrogenchloride / water / 48 h / 25 °C
2: AlCl3, aluminium chloride / 24 h / 25 °C / |Inert atmosphere
3: ammonium cerium (IV) nitrate / water; acetic acid / 2.25 h / 100 °C
View Scheme
参考文献
Ling, Xiaoxi; Masson, Eric
Organic Letters, 2012 , vol. 14, # 18 p. 4866 - 4869
反应条件
1: DMSO / 16 h / 180 °C
2: DMSO, H2O / 16 h / 180 °C
View Scheme
参考文献
Molnar, Arpad; Bartok, Mihaly
Helvetica Chimica Acta, 1981 , vol. 64, # 2 p. 389 - 398
反应条件
1: 89 percent / 37percent aq. HCl / 1 h
2: 60 percent Turnov. / AlCl3 / 1.67 h / 0 °C
3: 79 percent / Aliquat 336, 40percent aq. NaOH / 22 h / 80 °C
4: 68 percent / 90percent aq. formic acid / 6 h / Heating
View Scheme
参考文献
Mayr, Herbert; Heilmann, Werner; Baeuml, Engelbert; Vorbrueggen, Helmut
Chemische Berichte, 1991 , vol. 124, # 1 p. 203 - 206
参考文献
Hellier, Desmond G.; Liddy, H. Glendon
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 5 p. 431 - 436
反应条件
diethyl ether; phosphoric acid
参考文献
Paulson,D.R. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 9 p. 1783 - 1787
反应条件
hydrogen bromide; acetic acid
参考文献
Zelinsky
Chemische Berichte, 1902 , vol. 35, p. 2139
Full Text Show Details
Harries; Tuerk
Justus Liebigs Annalen der Chemie, 1905 , vol. 343, p. 366
参考文献
Engel, Paul S.; Robertson, Donald M.; Scholz, John N.; Shine, Henry J.
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6178 - 6187
