2,5-二甲基-2,5-己二醇合成路线 （共 107 条）
反应条件
aluminium trichloride T=55°C; 6 h;
参考文献
Held, Pierre; Heck, Marie-Pierre; Iyer, Jaya; Gronemeyer, Hinrich; Lebeau, Luc; Mioskowski, Charles
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 6 p. 501 - 507
反应条件
1: conc. HCl, HCl gas / 0.25 h / 0 °C 2: 81.9 percent / AlCl3 / 24 h / Heating View Scheme
参考文献
Selen Gurkan-Alp; Mumcuoglu, Mine; Andac, Cenk A.; Dayanc, Emre; Cetin-Atalay, Rengul; Buyukbingol, Erdem
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 346 - 354
→
22306-30-51,1,4,4,5,5,8,8-八甲基-1,2,3,4,5,6,7,8-八氢蒽
参考文献
Labanskii; Zukerwanik
Doklady Akademii Nauk SSSR, 1951 , vol. 80, p. 369,371
Chem.Abstr., 1952 , p. 5022
反应条件
aluminum oxide; phosphoric acid T=250°C;
参考文献
Kotljarewskii; Sanina
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1957 , vol. 30, p. 1356,1358; engl. Ausg. S. 1424, 1426
反应条件
pumice stone; zirconium oxide T=300°C;
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
参考文献
Bruson; Kroeger
Journal of the American Chemical Society, 1940 , vol. 62, p. 36,43
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
参考文献
Kotljarewskii; Sanina
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1957 , vol. 30, p. 1356,1358; engl. Ausg. S. 1424, 1426
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
反应条件
hydrogenchloride in water
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2007/5568 A1, 2007 ;
Location in patent: Page/Page column 10 ;
WO 2007/005568 A1
