2,5-二甲基-2,5-己二醇合成路线 （共 107 条）
参考文献
Henry
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1906 , vol. 143, p. 496
参考文献
Henry
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1906 , vol. 143, p. 496
反应条件
aluminum oxide T=350°C;
参考文献
Molnar, Arpad; Bartok, Mihaly
Helvetica Chimica Acta, 1981 , vol. 64, # 2 p. 389 - 398
反应条件
pumice stone; zirconium oxide T=300°C;
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
参考文献
Nasarow; Mawrow
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 3061,3064, 3069
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 3092,3094, 3099
反应条件
1: conc. HCl, HCl gas / 0.25 h / 0 °C 2: 81.9 percent / AlCl3 / 24 h / Heating 3: 49.9 percent / HNO3, H2SO4 / 1 h / -10 °C View Scheme
参考文献
Kagechika, Hiroyuki; Kawachi, Emiko; Hashimoto, Yuichi; Himi, Toshiyuki; Shudo, Koichi
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2182 - 2192
反应条件
1: glacial acetic acid; hydrogen chloride / und nachfolgenden Aufbewahren 2: soda lime / 255 - 270 °C / 12 - 20 Torr 3: 100 °C / im Rohr und Verseifen des Reaktionsprodukts mit alkoh. Kalilauge View Scheme
参考文献
Staudinger; Ruzicka
Helvetica Chimica Acta, 1924 , vol. 7, p. 385
反应条件
1: hydrogenchloride / ethanol 2: AlCl3, aluminium chloride 3: potassium permanganate / Alkaline conditions View Scheme
参考文献
Gurkan, A. Selen; Karabay, Arzu Z.; Buyukbingol, Zeliha; Buyukbingol, Erdem
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 2 p. 468 - 479
反应条件
1: HCl conc. / 3 h / 20 °C 2: 99 percent / AlCl3 / CH2Cl2 / 20 °C 3: 85 percent / Br2; AlCl3 / CH2Cl2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 17 p. 5772 - 5782
