反应条件
hydrogenchloride in toluene condensing gaseous HCl with liquid nitrogen in an ampul containing toluene solution of (((CH3)3Si)2N)2Yb*CH3O(CH2)2OCH3; warming to room temperature; removing volatile compounds ((CH3)3SiCl, DME) by vac. condensation; vac. sublimation at 100°C (1E-2 mm): NH4Cl;;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 55, p. 1911 - 1914
Zhurnal Obshchei Khimii, , vol. 55, p. 2153 - 2157