Dorokhov,V.A.; Mikhailov,B.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 340 - 341
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , # 2 p. 364 - 366
1: With palladium diacetate; 1,3-bis-(diphenylphosphino)propane; potassium carbonate in N,N-dimethyl-formamide
T=80°C;
2: With hydrogenchloride in N,N-dimethyl-formamide
1 h;
参考文献
LICA PHARMACEUTICALS A/S
Patent: WO2003/97575 A2, 2003 ;
Location in patent: Page/Page column 31 ;
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane
T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;