diethylaluminium chloride; zirconium tetrachloride in toluene T=120°C; 5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 6 p. 1132 - 1134
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1410 - 1412
1: oct-1-ene With 2,2'-azo-bisisobutyronitrile; O,O-diethyl phosphorothioite in tetrahydrofuran Heating; 2: methyl iodide With sec.-butyllithium in tetrahydrofuran; cyclohexane T=-78 - 20°C; 3: cyclohexanone With sec.-butyllithium in tetrahydrofuran; cyclohexane T=-78 - 20°C; Horner-Wadsworth-Emmons reaction; Title compound not separated from byproducts;
参考文献
Healy, Mark P.; Parsons, Andrew F.; Rawlinson, James G. T.
Organic Letters, 2005 , vol. 7, # 8 p. 1597 - 1600
[rhodium(I)chloride(triphenylphosphine)2]1 in acetonitrile-D3; benzene-d6 T=150°C; 0.166667 h; microwave irradiation;
参考文献
Mkhalid, Ibraheem A. I.; Coapes, R. Benjamin; Edes, S. Natasha; Coventry, David N.; Souza, Fabio E. S.; Thomas, Rhodri Ll.; Hall, Jonathan J.; Bi, Si-Wei; Lin, Zhenyang; Marder, Todd B.
Dalton Transactions, 2008 , # 8 p. 1055 - 1064
