1.1: manganese(IV) oxide; water / 120 - 135 °C / |Inert atmosphere
2.1: sodium methylate; bromine / methanol / 0.5 h / 0 - 5 °C
2.2: 55 - 60 °C
View Scheme
参考文献
Shapiro, Rafael; DiCosimo, Robert; Hennessey, Susan M.; Stieglitz, Barry; Campopiano, Onorato; Chiang, George C.
Organic Process Research and Development, 2001 , vol. 5, # 6 p. 593 - 598