1: With tri-isobutyl aluminium; bis-triphenylphosphine-palladium(II) chloride in dichloromethane T=25°C; 12 h; 2: With sodium hydroxide; oxygen in dichloromethane
1: With sodium tetrahydroborate; malonic acid; cyclohexene in tetrahydrofuran T=60°C; 5 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=40 - 50°C; 2 h; Further stages.;
参考文献
New Journal of Chemistry, , vol. 25, # 6 p. 869 - 871
hydrogen; (ethylenedinitrilo)tetraacetic acid disodium salt; iron(II) sulfate in water T=150°C; P=20686.5 Torr; 12 h; Title compound not separated from byproducts.;
