trichlorosilane; N-ethyl-N,N-diisopropylamine; copper(l) chloride in N,N-dimethyl-formamide
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Marshall, James A.; Adams, Nicholas D.
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 8976 - 8977
1.1: LDA / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: tetrahydrofuran; hexane / -78 °C
2.1: 10.6 g / CeCl3*7H2O; NaI / acetonitrile / 3 h / Heating
View Scheme
参考文献
Palomo, Claudio; Oiarbide, Mikel; Halder, Rajkumar; Kelso, Michael; Gomez-Bengoa, Enrique; Garcia, Jesus M.
Journal of the American Chemical Society, 2004 , vol. 126, # 30 p. 9188 - 9189
1: diethyl ether / 0 - 25 °C
2: thionyl chloride (excess) / diethyl ether / 0 - 25 °C
3: 48 percent / NaI / acetone
View Scheme
参考文献
Smith, Janice Gorzynski; Drozda, Susan E.; Petraglia, Susan P.; Quinn, Nina R.; Rice, Elizabeth M.; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4112 - 4120
