反应条件
1: 1.) N,N,N',N'-tetramethylenediamine, n-BuLi / 1.) 4 h, -78 degC, THF; 2.) THF, -78 degC, 30 min
2: 1.) N-chlorosuccinimide, AgNO3, NaHCO3; 2.) NaBH4 / 1.) MeCN, water, 40-45 degC, 15 min; 2.) water, 15 min
View Scheme
参考文献
Ko, Kwang-Youn; Frazee, William J.; Eliel, Ernest L.
Tetrahedron, 1984 , vol. 40, # 8 p. 1333 - 1344
