反应条件
1: 1.) B2H6, 2.) H2O2/3N NaOH / 1.) diglyme, 5h, 2.) room temperature, overnight
2: 85 percent / PBr3 / benzene / 5 h / Ambient temperature
3: 22 g / acetonitrile / 8 h / Heating
4: 1.) potassium tert-butanolate / 1.) DMF, 20 deg C, 3h, 2.) 5h
5: LiAlH4 / diethyl ether / 3 h / Heating
6: pyridine / 10 h / Ambient temperature
View Scheme
参考文献
Dzhemilev, U. M.; Balezina, G. G.; Volkova, L. A.; Krivonogov, V. P.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1980 , vol. 16, # 1 p. 82 - 85
Khimiya Prirodnykh Soedinenii, 1980 , vol. 16, # 1 p. 97 - 102
