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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
壬烷
合成路线
（共 222 条）
693-03-8
溴丁基-镁
+
507-19-7
溴代叔丁烷
+
110-53-2
溴代正戊烷
→
反应条件
590-73-8
2,2-二甲基己烷
+
111-84-2
壬烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With n-butyl-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 1-bromo-1,1-dimethylethane; n-bromopentane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
78-77-3
溴代异丁烷
+
110-53-2
溴代正戊烷
→
反应条件
592-27-8
2-甲基庚烷
+
111-84-2
壬烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: 2-methyl-1-bromopropane; n-bromopentane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
111-83-1
溴辛烷
→
反应条件
111-84-2
壬烷
+
112-40-3
正十二烷
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; 1-bromo-octane in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
100-39-0
溴化苄
→
反应条件
111-84-2
壬烷
+
538-68-1
戊基苯
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With (4-Methylphenyl)-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; benzyl bromide in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 12 p. 1148 - 1154
693-03-8
溴丁基-镁
+
110-53-2
溴代正戊烷
+
103-63-9
(2-溴乙基)苯
→
反应条件
111-84-2
壬烷
+
1077-16-3
己基苯
反应条件
1: n-butyl-magnesium bromide With copper(l) iodide in tetrahydrofuran T=-20°C; 0.0333333 h; Inert atmosphere; 2: With n-butyl-magnesium bromide in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-bromopentane; 2-(phenyl)ethyl bromide in tetrahydrofuran T=-20 - 25°C; Inert atmosphere; Kinetics; Reagent/catalyst;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 12 p. 1148 - 1154
17463-01-3
壬-2-烯酸乙酯
→
反应条件
111-84-2
壬烷
+
4468-61-5
反应条件
Multistep reaction;
参考文献
Tetrahedron Letters, , p. 3337 - 3340
112-13-0
→
反应条件
111-84-2
壬烷
反应条件
trichlorosilane in neat (no solvent) Ambient temperatureIrradiationother acid chlorides with primary alkyl; Product distributionMechanism;
参考文献
Oka, Kunio; Nakao, Ren; Abe, Yasuo; Dohmaru, Takaaki
Journal of Organometallic Chemistry, 1990 , vol. 381, # 2 p. 155 - 164
111-65-9
正辛烷
→
反应条件
111-84-2
壬烷
+
124-18-5
+
1120-21-4
+
112-40-3
正十二烷
+
629-62-9
正十五烷
+
74-84-0
乙烷
+
142-82-5
+
629-50-5
十三烷
+
629-59-4
+
544-76-3
正十六烷
反应条件
hexamethyl-benzene; C24H42IrO3P2(1-)*K(1+); Re2O7/Al2O3 T=50 - 220°C; 52 h; Inert atmosphereTwo-pot reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 1 p. 125 - 135
111-65-9
正辛烷
→
反应条件
111-84-2
壬烷
+
124-18-5
+
1120-21-4
+
112-40-3
正十二烷
+
74-98-6
丙烷
+
110-54-3
正己烷
+
142-82-5
+
629-50-5
十三烷
+
106-97-8
+
109-66-0
反应条件
hexamethyl-benzene; C24H42IrO3P2(1-)*K(1+); Re2O7/Al2O3 T=50 - 220°C; 52 h; Inert atmosphereTwo-pot reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 1 p. 125 - 135
124-18-5
→
反应条件
111-65-9
正辛烷
+
111-84-2
壬烷
+
1120-21-4
+
112-40-3
正十二烷
+
74-84-0
乙烷
+
74-98-6
丙烷
+
110-54-3
正己烷
+
142-82-5
+
106-97-8
+
109-66-0
反应条件
C32H60IrO3P3; Re2O7/Al2O3; 1,3,5-trimethyl-benzene T=175°C; 168 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 1 p. 125 - 135
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