(R)-(+)-β-香茅醇合成路线 （共 81 条）
反应条件
Produkt5: Oxalsaeure;
参考文献
Fester; Bertuzzi; Pucci
Chemische Berichte, 1937 , vol. 70, p. 40
反应条件
jones reagent T=20°C; Oxidation; Jones oxidation; 2 h;
参考文献
Yabuuchi, Tetsuya; Kusumi, Takenori
Journal of Organic Chemistry, 2000 , vol. 65, # 2 p. 397 - 404
参考文献
Tiemann; Schmidt
Chemische Berichte, 1897 , vol. 30, p. 27
Chemische Berichte, 1896 , vol. 29, p. 913
参考文献
Ciba-Geigy AG
Patent: US4661601 A1, 1987 ;
反应条件
1: <RuCl2((S)-(-)-tol-binap)>2*Et3N / methanol / 2 h / 19.9 °C 2: H2, <RuCl2((S)-(-)-tol-binap)>2*Et3N / methanol / 19.9 °C / 3750.3 Torr View Scheme
参考文献
Sun, Yongkui; LeBlond, Carl; Wang, Jian; Blackmond, Donna G.; Laquidara, Joseph; Sowa Jr., John R.
Journal of the American Chemical Society, 1995 , vol. 117, # 50 p. 12647 - 12648
反应条件
(i) NaH, CS2, THF, (ii) MeI, (iii) (heating); Multistep reaction;
参考文献
Cernigliaro,G.J.; Kocienski,P.J.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3622 - 3624
反应条件
1: 15 mg / SeO2 / ethanol / 2 h / Heating 2: AgNO3, 10 percent aq. NaOH / Ambient temperature View Scheme
参考文献
Miyase; Akahori; Kohsaka; Ueno
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 11 p. 2944 - 2951
反应条件
in dichloromethane T=25°C; 0.25 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5152 - 5155
反应条件
1: dihydrogen peroxide; sodium bromide / tert-butyl alcohol / 1 h / 25 °C / pH 3.6 / aq. buffer; Enzymatic reaction 2: potassium tert-butylate / dimethyl sulfoxide / 100 °C View Scheme
参考文献
Piantini, Umberto; Schrader, Jens; Wawrzun, Andrzej; Wuest, Matthias
Food Chemistry, 2011 , vol. 129, # 3 p. 1025 - 1029
参考文献
Tiemann; Schmidt
Chemische Berichte, 1896 , vol. 29, p. 921,924
Chemische Berichte, 1897 , vol. 30, p. 38
