反应条件
water; sodium acetate in water
addn. of soln. of NaOAc to soln. of BuSnCl3 to pH = 1.5, addn. of solid W-Bi salt, (stirring), filtration after 10 min, addn. of KCl into filtr ate (pptn.); filtration, drying (vac., 1 h), washing (satd. soln. of KCl), drying (vac., overnight), recrystn. (vapor diffusion of EtOH); elem. anal.;
参考文献
Rusu, Mariana; Tomsa, Adrian R.; Rusu, Dan; Haiduc, Ionel
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 6 p. 951 - 965
