反应条件
1: 1) Li, liq.NH3, Fe(NO3)3 / 1) THF, 1 h, 2) THF, 2 h 2: 95 percent / H2 / Lindlar's catalyst / hexane 3: 90 percent / NEt3 / CH2Cl2 / 0 °C 4: 1) Mg, 2) HMPA / 1) THF, 2) THF, r.t., overnight 5: 60 percent / m-chloroperbenzoic acid / CH2Cl2 / 1) 0 deg C, 45 min, 2) r.t., 30 min View Scheme
参考文献
Jonas, Jaroslav; Slanina, Pavel; Humpa, Otakar; Mazal, Ctibor
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 4 p. 857 - 859
