反应条件
2: 0.1 M aq. p-toluenesulfonic acid / tetrahydrofuran / 0.3 h / Heating
3: 1.) NaN(SiMe3)2 / 1.) THF, toluene, r.t., 1 h 2.) THF, -100 deg C to 0 deg C
4: 0.1 M aq. p-toluenesulfonic acid / tetrahydrofuran / 0.3 h / Heating
5: 1.) LiAlH4 2.) 2N HCl, H2O / 1.) THF, -70 deg C 2.) -20 deg C
6: 95 percent / CBr4, triphenylphosphine / CH2Cl2 / -5 °C
View Scheme
参考文献
Viala; Munier; Santelli
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3347 - 3352
