2,2'-azo-bisisobutyronitrile in benzene Refluxing in benzene (8 h, N2) after addn. of AIBN as a free radical initiator, quenching of react. mixt. by cooling in ice bath.; GLC anal. with n-dodecane as an added integration std.;
参考文献
Pike, Philip W.; Gilliatt, Vernon; Ridenour, Michael; Hershberger, James W.
Organometallics, 1988 , vol. 7, p. 2220 - 2223
2,2'-azo-bisisobutyronitrile in benzene Refluxing in benzene (8 h, N2) after addn. of AIBN as a free radical initiator, quenching of react. mixt. by cooling in ice bath.; GLC anal. with n-dodecane as an added integration std.;
参考文献
Pike, Philip W.; Gilliatt, Vernon; Ridenour, Michael; Hershberger, James W.
Organometallics, 1988 , vol. 7, p. 2220 - 2223
