in benzene in presence of NaBPh4, stirring for several h; pptn. on water addn., collection, sublimation off of W(CO)6 (vac., 50°C), extn. into hexane, recrystn. (hexane); elem. anal.;
参考文献
Meester, M. A. M.; Vriends, R. J. C.; Stufkens, D. J.; Vrieze, K.
Inorganica Chimica Acta, 1976 , vol. 19, p. 95 - 104