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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-碘吡啶
合成路线
（共 228 条）
1120-90-7
3-碘吡啶
+
99-90-1
4-溴苯乙酮
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
1: para-bromoacetophenone With indium; bathophenanthroline; 3-chloroprop-1-ene; lithium chloride; cobalt(II) dibromide in tetrahydrofuran T=100°C; 15 h; Inert atmosphere; 2: 3-iodo-pyridine With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=80°C; 18 h; Inert atmosphere;
参考文献
Adak, Laksmikanta; Yoshikai, Naohiko
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7563 - 7568
1120-90-7
3-碘吡啶
+
619-44-3
4-碘苯甲酸甲酯
→
反应条件
90395-47-4
4-(3-吡啶)苯甲酸甲酯
反应条件
1: 3-iodo-pyridine With i -Pr2Zn; Li(acac) in 1-methyl-pyrrolidin-2-one T=20°C; 12 h; 2: 4-iodo-benzoic acid methyl ester With trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; Negishi cross-coupling reaction; 12 h;
参考文献
Gong, Liu-Zhu; Knochel, Paul
Synlett, 2005 , # 2 art. no. G41404ST, p. 267 - 270
1120-90-7
3-碘吡啶
+
93-58-3
苯酸甲酯
→
反应条件
90395-46-3
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
1120-90-7
3-碘吡啶
+
16419-60-6
2-甲基苯硼酸
→
反应条件
90395-49-6
反应条件
sodium carbonate in water; ethyl acetate; isopropyl alcohol T=50°C; Suzuki-Miyaura coupling; 0.00138889 h; Microchannel flow reactor;
参考文献
Yamada, Yoichi M. A.; Watanabe, Toshihiro; Beppu, Tomohiko; Fukuyama, Naoshi; Torii, Kaoru; Uozumi, Yasuhiro
Chemistry - A European Journal, 2010 , vol. 16, # 37 p. 11311 - 11319
1120-90-7
3-碘吡啶
+
108-88-3
甲苯
→
反应条件
4423-09-0
3-(4-甲基苯基)吡啶
+
90395-49-6
+
4385-67-5
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
1120-90-7
3-碘吡啶
+
519059-04-2
→
反应条件
918542-10-6
反应条件
triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=20 - 60°C; 1 h;
参考文献
Wyeth
Patent: US2007/4730 A1, 2007 ;
Location in patent: Page/Page column 26 ;
US 20070004730 A1
110-91-8
吗啉
+
1120-90-7
3-碘吡啶
→
反应条件
2767-91-1
4-吗啉吡啶
+
92670-29-6
反应条件
iron(III) oxide; L-proline; sodium t-butanolate in dimethyl sulfoxide T=135°C; 24 h;
参考文献
Quo, Diliang; Huang, He; Xu, Jinyi; Jiang, Hualiang; Liu, Hong
Organic Letters, 2008 , vol. 10, # 20 p. 4513 - 4516
1120-90-7
3-碘吡啶
+
1666-13-3
→
反应条件
94800-54-1
反应条件
copper(I) oxide; [2,2']bipyridinyl; magnesium in N,N-dimethyl-formamide T=110°C; 18 h;
参考文献
Taniguchi, Nobukazu; Onami, Tetsuo
Synlett, 2003 , # 6 p. 829 - 832
Title/Abstract Full Text View citing articles Show Details
Taniguchi, Nobukazu; Onami, Tetsuo
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 915 - 920
1120-90-7
3-碘吡啶
+
108-90-7
→
反应条件
5957-97-1
+
5970-10-5
+
4381-37-7
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
1120-90-7
3-碘吡啶
+
108-88-3
甲苯
→
反应条件
4423-09-0
3-(4-甲基苯基)吡啶
+
90395-49-6
+
4385-67-5
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Ohkura, Kazue; Seki, Koh-ichi; Terashima, Masanao; Kanaoka, Yuichi
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3433 - 3436
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