2-巯基吡啶-N-氧化物合成路线 （共 16 条）
反应条件
in acetone
K2(PtCl4) and 1-oxidopyridinium-2-thiol heated under reflux in acetone for 1 h; product filtered off; elem. anal.;
参考文献
Davidson, Jack L.; Preston, Peter N.; Russo, Maria V.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 783 - 786
反应条件
in acetone
1-oxidopyridinium-2-thiol added to stirred soln. Zeise's salt in acetone at room temp.; ppt. washed with hot chloroform, filtrate evapd.;
参考文献
Davidson, Jack L.; Preston, Peter N.; Russo, Maria V.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 783 - 786
反应条件
in water
K2(PtCl4), 1-oxidopyridinium-2-thiol and water stirred at room temp. for 1 h; ppt. washed with acetone and Et2O (filtrate - bis(1-oxidopyridinium-2-thiolato)platinum(II)), then with chloroform, acetone and water; elem. anal.;
参考文献
Davidson, Jack L.; Preston, Peter N.; Russo, Maria V.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 783 - 786
反应条件
dicyclohexyl-carbodiimide in dichloromethane
T=25°C; 10 h;
参考文献
Ling, Taotao; Poupon, Erwan; Rueden, Erik J.; Kim, Sun H.; Theodorakis, Emmanuel A.
Journal of the American Chemical Society, 2002 , vol. 124, # 41 p. 12261 - 12267
反应条件
N-chloro-succinimide in toluene
参考文献
SmithKline Beckman Corporation
Patent: US4505917 A1, 1985 ;
反应条件
1: 81 percent / H2O2 / H2O / 1 h / 45 °C
2: HOAc / CH2Cl2 / 30 h / Ambient temperature
3: 89 percent / CHCl3 / 18 h / Ambient temperature
View Scheme
参考文献
Barton, Derek H. R.; Chen, Chen; Wall, G. Michael
Tetrahedron, 1991 , vol. <32> 47, p. 6127 - 6138
