1,4-二甲基-2-碘苯合成路线 (共 37 条)
反应条件
hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI;
参考文献
Monatshefte fuer Chemie, , vol. 64, p. 361,364, 365
Monatshefte fuer Chemie, , vol. 65, p. 6,14
反应条件
in acetonitrile-D3 T=45°C; Inert atmosphereDarkness; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 24 p. 4079 - 4083
反应条件
T=25°C; Dissoziation; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2374,2376
反应条件
trans-[PdBr(Ph)(PPh3)2]; iodine T=120°C; 2 h; other hydrocarbons; also with Br2; var. temp. and time; Product distribution;
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 11.1 p. 1767 - 1776
Zhurnal Organicheskoi Khimii, , vol. 29, # 11 p. 2129 - 2140
参考文献
Chemische Berichte, , vol. 33, p. 2884
参考文献
Journal of the Indian Chemical Society, , vol. 13, p. 187
Gazzetta Chimica Italiana, , vol. 71, p. 297,299
Journal of the Indian Chemical Society, , vol. 12, p. 343
反应条件
sodium hydroxide; hydrazine hydrate; mercury dichloride; palladium dichloride 6 h; Heating;
参考文献
Nakajima, Riichiro; Shintani, Yuji; Hara, Tadashi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1767 - 1768
反应条件
1: NH3, O2, H2O / Sn-V catalyst / 380 - 420 °C 2: aq. NaOH View Scheme
参考文献
Suvorov,B.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 1547 - 1550
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, p. 1609 - 1613
反应条件
1: With copper(l) iodide; 2-methyl-8-hydroxyquinoline; tetra(n-butyl)ammonium hydroxide in water; dimethyl sulfoxide T=100°C; 10 h; 2: With hydrogenchloride in water; N,N-dimethyl-formamide T=20°C;
参考文献
Paul, Rajesh; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Synthesis, 2010 , # 24 art. no. P11610SS, p. 4268 - 4272
反应条件
[(PPh3)3Pd] in tetrahydrofuran T=22°C; 48 h; other reagent, reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 62, # 25 p. 8957 - 8960