3,5-二甲基-2-环己烯-1-酮合成路线 （共 86 条）
反应条件
1: methyl-magnesium iodide With copper(l) chloride in diethyl ether complexation; 0.0833333 h; cooling; 2: 3,5-dimethyl-cyclohex-2-en-1-one in diethyl ether Addition; 1 h; cooling;
参考文献
Jirgensons, Aigars; Kauss, Valerjans; Kalvinsh, Ivars; Gold, Markus R.; Danysz, Wojciech; Parsons, Chris G.; Quack, Gunter
European Journal of Medicinal Chemistry, 2000 , vol. 35, # 6 p. 555 - 565
反应条件
hydrogen; Rhodium chloride tri(triphenylphosphine-meta-trisulfonate) in water 17 h; Ambient temperature;
参考文献
Larpent, Chantal; Dabard, Renee; Patin, Henri
Tetrahedron Letters, 1987 , vol. 28, # 22 p. 2507 - 2510
反应条件
lithium n-butyldiisobutylaluminum hydride; (2,6-t-Bu2-4-Me-C6H2O)2AlMe in diethyl ether; hexane; toluene T=-78°C; 0.25 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 2241 - 2243
反应条件
p-mentha-1,8-diene; palladium on activated charcoal 0.5 h; Heating;
参考文献
Holleben, Maria Luiza A. von; Zucolotto, Monica; Zini, Claudia A.; Oliveira, Eduardo R.
Tetrahedron, 1994 , vol. 50, # 4 p. 973 - 978
反应条件
sodium tetrahydroborate; SmCpCl2(THF)3 in methanol 6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Komiya, Sanshiro; Tsutsumi, Osamu
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3423 - 3424
反应条件
T=200°C; P=75 - 80 Torr;
参考文献
Zelinsky
Chemische Berichte, 1911 , vol. 44, p. 2779
反应条件
Behandeln mit Zinkstaub;
参考文献
Knoevenagel
Justus Liebigs Annalen der Chemie, 1897 , vol. 297, p. 183
反应条件
ammonium cerium(IV) nitrate; iodine 7 h; Heating;
参考文献
Horiuchi, C. Akira; Fukunishi, Hirotada; Kajita, Mika; Yamaguchi, Akihisa; Kiyomiya, Hiroshi; Kiji, Shinji
Chemistry Letters, 1991 , # 11 p. 1921 - 1924
反应条件
titanium tetrachloride; Me3SnLi 1.) THF, 0 deg C, 15 min, 2.) CH2Cl2, -78 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Watanabe, Masami; Watanabe, Toshiyuki; Onoda, Yasuo; Murayama, Eigoro
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 1894 - 1899
反应条件
hydrogenchloride; ethanol Behandeln des Reaktionsprodukts mit HCl in Aether und Erhitzen der erhaltenen Hydrochloride unter vermindertem Druck auf 200-235grad;
参考文献
Journal of Organic Chemistry, , vol. 9, p. 552,554
