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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丙酮酸钠
合成路线
（共 123 条）
113-24-6
丙酮酸钠
→
反应条件
50-21-5
乳酸
反应条件
lactic dehydrogenase; lipoamide dehydrogenase in water Ambient temperatureIrradiationpH=7.5; Title compound not separated from byproducts;
参考文献
Mandler, Daniel; Willner, Itamar
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 805 - 812
113-24-6
丙酮酸钠
+
108-95-2
苯酚
→
反应条件
35424-81-8
L-酪氨酸-15N
反应条件
15N-ammonium sulfate in water T=37°C; bacterial cells Erwinia herbicola, pH 8.5;
参考文献
Walker, T. E.; Matheny, C.; Storm, C. B.; Hayden, H.
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1175 - 1179
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
73-22-3
L-色氨酸
→
反应条件
146142-94-1
莽那亭
反应条件
potassium phosphate; pyridoxal 5'-phosphate; magnesium chloride; Comamonas testosteroni proA Aldolase; HIS6-HEXaspC aminotransferase in water T=30°C; pH=7.8; 21 - 29 h; Enzymatic reaction; Product distribution / selectivity;
参考文献
Cargill, Incorporated
Patent: US2008/15361 A1, 2008 ;
Location in patent: Page/Page column 26 ;
113-24-6
丙酮酸钠
+
100-52-7
苯甲醛
→
反应条件
1798-60-3
(R)-1-羟基-1-苯基丙酮
+
513-86-0
3-羟基-2-丁酮
反应条件
pyruvate decarboxylase in octanol; water T=4°C; pH=6.5 - 8; 40 - 395 h; Enzymatic reactionaqueous MOPS buffer; Product distribution / selectivity;
参考文献
BASF Aktiengesellschaft
Patent: US7074966 B2, 2006 ;
Location in patent: Page/Page column 4-5 ;
113-24-6
丙酮酸钠
+
91-56-5
吲哚-2,3-二酮
→
反应条件
486-74-8
喹啉-4-羧酸
反应条件
1: With water; sodium hydroxide T=110°C; Pfitzinger reaction; P=4500.45 Torr; 0.166667 h; Microwave irradiation; 2: in water T=190 - 200°C; Pfitzinger reaction; P=12001.2 - 13501.4 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Zhu, Hui; Yang, Ri Fang; Yun, Liu Hong; Li, Jin
Chinese Chemical Letters, 2010 , vol. 21, # 1 p. 35 - 38
113-24-6
丙酮酸钠
→
反应条件
50-21-5
乳酸
反应条件
lactic dehydrogenase; lipoamide dehydrogenase in water Ambient temperatureIrradiationpH=7.5; Title compound not separated from byproducts;
参考文献
Mandler, Daniel; Willner, Itamar
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 805 - 812
22374-89-6
1-甲基-3-苯基丙胺
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
2550-26-7
苄基丙酮
+
4187-57-9
(S)-(+)-1-甲基-3-苯基丙胺
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
113798-74-6
2,3,6-三氟苯酚
→
反应条件
182756-60-1
反应条件
ammonium acetate; tyrosine phenol lyase; 2-hydroxyethanethiol; pyridoxal 5'-phosphate T=20°C; pH=8.0;
参考文献
Seyedsayamdost, Mohammad R.; Reece, Steven Y.; Nocera, Daniel G.; Stubbe, JoAnne
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1569 - 1579
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