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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丙酮酸钠
合成路线
（共 123 条）
443-69-6
5-氟靛红
+
113-24-6
丙酮酸钠
→
反应条件
220844-73-5
6-氟喹啉-4-羧酸
反应条件
1: With water; sodium hydroxide T=110°C; Pfitzinger reaction; P=4500.45 Torr; 0.166667 h; Microwave irradiation; 2: in water T=190 - 200°C; Pfitzinger reaction; P=12001.2 - 13501.4 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Zhu, Hui; Yang, Ri Fang; Yun, Liu Hong; Li, Jin
Chinese Chemical Letters, 2010 , vol. 21, # 1 p. 35 - 38
2268-15-7
2,3,5-三氟苯酚
+
113-24-6
丙酮酸钠
→
反应条件
182756-63-4
反应条件
ammonium acetate; tyrosine phenol lyase; 2-hydroxyethanethiol; pyridoxal 5'-phosphate T=20°C; pH=8.0;
参考文献
Seyedsayamdost, Mohammad R.; Reece, Steven Y.; Nocera, Daniel G.; Stubbe, JoAnne
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1569 - 1579
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
338-69-2
D-丙氨酸
+
2627-86-3
(S)-(-)- α-甲基苄胺
+
3886-69-9
R(+)-alpha-甲基苄胺
+
98-86-2
苯乙酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
56-41-7
氨基丙酸
+
3886-69-9
R(+)-alpha-甲基苄胺
+
98-86-2
苯乙酮
反应条件
(S)-selective ω-transaminase from Ochrobactrum anthropi; pyridoxal 5'-phosphate T=37°C; pH=7.5; 3 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Malik, M. Shaheer; Park, Eul-Soo; Shin, Jong-Shik
Green Chemistry, 2012 , vol. 14, # 8 p. 2137 - 2140
113-24-6
丙酮酸钠
→
反应条件
127-17-3
丙酮酸
反应条件
hydrogenchloride; water in acetonitrile T=0 - 20°C; 3 h; Product distribution / selectivity;
参考文献
AMERSHAM HEALTH AS
Patent: WO2006/38811 A1, 2006 ;
Location in patent: Page/Page column 7-8 ;
120-72-9
吲哚
+
113-24-6
丙酮酸钠
→
反应条件
73-22-3
L-色氨酸
反应条件
ammonia; pyridoxal 5'-phosphate in a continuous flow reactor containing Escherichia coli cells in polyacrylamide gel;
参考文献
Azerad; Calderon Seguin; Decottignies Le Marechal
Bulletin de la Societe Chimique de France, 1980 , vol. II, # 1-2 p. 83 - 86
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
338-69-2
D-丙氨酸
+
2627-86-3
(S)-(-)- α-甲基苄胺
+
98-86-2
苯乙酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; Reagent/catalyst; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
338-69-2
D-丙氨酸
+
2627-86-3
(S)-(-)- α-甲基苄胺
+
3886-69-9
R(+)-alpha-甲基苄胺
+
98-86-2
苯乙酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
403-40-7
1-(4-氟苯基)乙胺
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
403-42-9
4-氟苯乙酮
+
66399-30-2
(S)-(-)-1-(4-氟苯基)乙胺
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
22374-89-6
1-甲基-3-苯基丙胺
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
2550-26-7
苄基丙酮
+
4187-57-9
(S)-(+)-1-甲基-3-苯基丙胺
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
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