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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丙酮酸钠
合成路线
（共 123 条）
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
338-69-2
D-丙氨酸
+
2627-86-3
(S)-(-)- α-甲基苄胺
+
98-86-2
苯乙酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; Reagent/catalyst; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
618-36-0
α-苯乙胺
→
反应条件
338-69-2
D-丙氨酸
+
2627-86-3
(S)-(-)- α-甲基苄胺
+
3886-69-9
R(+)-alpha-甲基苄胺
+
98-86-2
苯乙酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
→
反应条件
56-41-7
氨基丙酸
+
338-69-2
D-丙氨酸
反应条件
alanine dehydrogenase; lipoamide dehydrogenase in water Ambient temperatureIrradiationpH=7.9; Title compound not separated from byproducts;
参考文献
Levine, Mindy; Kenesky, Craig Scott; Mazori, Daniel; Breslow, Ronald
Organic Letters, 2008 , vol. 10, # 12 p. 2433 - 2436
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
反应条件
transaminase ATA-117; (R)-1-phenyl-ethyl-amine Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Hopwood, Jennifer; Truppo, Matthew D.; Turner, Nicholas J.; Lloyd, Richard C.
Chemical Communications, 2011 , vol. 47, # 2 p. 773 - 775
403-40-7
1-(4-氟苯基)乙胺
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
403-42-9
4-氟苯乙酮
+
66399-30-2
(S)-(-)-1-(4-氟苯基)乙胺
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
113-24-6
丙酮酸钠
+
108-95-2
苯酚
→
反应条件
60-18-4
L-酪氨酸
反应条件
ammonium sulfate; tyrosine phenol lyase; ammonium chloride in diethyl ether T=30°C; pH=8; aq. phosphate buffer;
参考文献
Seisser, Birgit; Zinkl, Rene; Gruber, Karl; Kaufmann, Franz; Hafner, Andreas; Kroutil, Wolfgang
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 4 p. 731 - 736
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
34698-41-4
1-氨基茚满
+
113-24-6
丙酮酸钠
→
反应条件
338-69-2
D-丙氨酸
+
10277-74-4
(R)-(-)-1-氨基茚满
+
83-33-0
1-茚酮
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
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