3,4-二甲氧基苯乙酮合成路线 (共 188 条)
反应条件
water; 2-nitro-4,5-dichloropyridazin-3(2H)-one in methanol T=150°C; P=10336 Torr; 0.166667 h; Microwave irradiation;
参考文献
Kim, Bo Ram; Lee, Hyung-Geun; Kim, Eun Jung; Lee, Sang-Gyeong; Yoon, Yong-Jin
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 484 - 486
反应条件
potassium dichromate; aluminium trichloride 0.05 h;
参考文献
Mohammadpoor-Baltork, Iraj; Sadeghi, Majid M.; Adibi, Abol-Hassan
Molecules, 2001 , vol. 6, # 11 p. 900 - 908
反应条件
silver perchlorate; niobium pentachloride in nitromethane T=80°C; Friedel-Crafts acylation; 1 h;
参考文献
Arai, Shigeru; Sudo, Yukinori; Nishida, Atsushi
Tetrahedron, 2005 , vol. 61, # 19 p. 4639 - 4642
反应条件
aluminium trichloride; sulfur dioxide
参考文献
Industrial and Engineering Chemistry, , vol. 34, p. 924
反应条件
oxygen; caesium carbonate; (-)-sparteine; PdCl2(nbd); 3 A molecular sieve in toluene; tert-butyl alcohol T=40°C; P=760 Torr; 18 h;
参考文献
Organic letters, , vol. 5, # 6 p. 835 - 837
反应条件
aluminum oxide; trifluoroacetic anhydride 0.416667 h; Ambient temperature;
参考文献
Ranu, Brindaban C.; Ghosh, Keya; Jana, Umasish
Journal of Organic Chemistry, 1996 , vol. 61, # 26 p. 9546 - 9547
反应条件
benzyltriphenylphosphonium dichromate in acetonitrile Oxidation; 0.5 h; Heating;
参考文献
Hajipour; Mallakpour
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 356, p. 371 - 387
反应条件
potassium carbonate in acetone T=65 - 70°C;
参考文献
US2010/168180 A1, ;
Page/Page column 10 ;
US 20100168180 A1
反应条件
perchloric acid; oxygen; palladium diacetate; p-benozquinone; sodium nitrite in methanol; water T=20°C; Wacker Oxidation; 24 h; Schlenk techniqueSealed tubeGreen chemistry;
参考文献
Zhang, Guofu; Xie, Xiaoqiang; Wang, Yong; Wen, Xin; Zhao, Yun; Ding, Chengrong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2947 - 2950
反应条件
benzyltriphenylphosphonium dichromate; silica gel 0.25 h;
参考文献
Hajipour; Mallakpour
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 356, p. 371 - 387