3,4-二甲氧基苯乙酮合成路线 （共 188 条）
反应条件
1: 0.91 g / diethyl ether / 0.75 h 2: 0.58 g / CrO3/conc. H2SO4 / H2O; acetone / 1 h / 5 - 10 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3024 - 3038
反应条件
1: 70 percent / pyridinium chlorochromate / CH2Cl2 / 10 h / 30 °C 2: aqueous sodium hydroxide (10percent) / methanol / 2 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1323 - 1324
反应条件
Bacillus coagulans NCIMB 9365 T=30°C; pH=7; 6 h; aq. phosphate bufferResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 63, # 1-2 p. 87 - 92
反应条件
1: 86 percent / sodium acetate / aq. ethanol / 6 h / Heating 2: 67 percent / aq. KOH / 40 h / Ambient temperature 3: conc. HCl / 0.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2477 - 2486
反应条件
1: KOH, Aliquat 336 2: AlCl3 / CH2Cl2 View Scheme
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 161, p. 395 - 402
反应条件
Aspergillus oryzae MIM T=30°C; pH=7; 6 h; aq. phosphate bufferResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 63, # 1-2 p. 87 - 92
反应条件
1.1: sodium iodide / acetone / 0.17 h / 20 °C 1.2: 20 °C 2.1: isopropyl alcohol / 15 h / Irradiation; Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 20 p. 8232 - 8242
反应条件
aluminum tri-bromide in 1,2-dichloro-benzene 22 h; Ambient temperaturevarious amounts of AlBr3; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 102, # 9 p. 3056 - 3062
反应条件
molybdenum hexacarbonate in acetonitrile 48 h; Heating;
参考文献
Russian Journal of Organic Chemistry, , vol. 40, # 7 p. 1003 - 1008
反应条件
Ce-Clay T=100°C; 1 - 5 h;
参考文献
Council of Scientific and Industrial Research
Patent: US6730814 B1, 2004 ;
Location in patent: Page column 7 - 8 ;
