3,4-二甲氧基苯乙酮合成路线 （共 188 条）
参考文献
Chemische Berichte, , vol. 70, p. 190,193
参考文献
Journal of the Chemical Society, , vol. 105, p. 1051
反应条件
1: POCl3 / 20 °C 2: NaOH / dioxane; H2O / 20 °C View Scheme
参考文献
Kotha, Sambasivarao; Seema, Vittal
Synlett, 2011 , # 16 art. no. D16111ST, p. 2329 - 2334
反应条件
4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; ammonium formate in methanol T=80°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Talwar, Dinesh; Salguero, Noemi Poyatos; Robertson, Craig M.; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 245 - 252
反应条件
1: in tetrahydrofuran; methanol T=0°C; 0.0833333 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=0°C; 6 h;
参考文献
Zhang, Wei; Zhang, Wenxue; Dai, Yisi; Zhu, Haizhen
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1747 - 1750
参考文献
Mannich
Archiv der Pharmazie (Weinheim, Germany), 1910 , vol. 248, p. 143
Chem. Zentralbl., 1909 , vol. 80, # I p. 923
反应条件
hydrogen bromide 3 h; Heating;
参考文献
RICHTER GEDEON VEGYESZETI GYAR RT.
Patent: WO2006/61666 A2, 2006 ;
Location in patent: Page/Page column 22-23 ;
反应条件
2-F-octylethanethiol; potassium tert-butylate in N,N-dimethyl-formamide T=110°C; 2 h; Inert atmosphere;
参考文献
Kale, Bhima; Shinde, Ananta; Sonar, Swapnil; Shingate, Bapurao; Kumar, Sanjeev; Ghosh, Samir; Venugopal, Soodamani; Shingare, Murlidhar
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3075 - 3078
反应条件
1: sodium hydride / tetrahydrofuran / 18 h / 20 °C / Reflux 2: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 100 °C / under air View Scheme
参考文献
Zhao, Jie; Zhao, Yufen; Fu, Hua
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3769 - 3773
反应条件
1: sodium hydride / tetrahydrofuran / 18 h / 20 °C / Reflux 2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C / under air View Scheme
参考文献
Zhao, Jie; Zhao, Yufen; Fu, Hua
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3769 - 3773
