3,5-二甲氧基苯甲酸合成路线 （共 127 条）
反应条件
sulfuric acid in chloroform
参考文献
Laatsch; Anke
1982 , vol. No. 12, p. 2189 - 2215
反应条件
ammonia; lithium in methanol
参考文献
Masaguer, Christian F.; Casariego, Isabel; Ravina, Enrique
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 5 p. 621 - 632
反应条件
1.1: LiAlH4 / tetrahydrofuran / 3 h / 20 °C 1.2: 97 percent / Na/K tartrate / tetrahydrofuran / 1 h / 20 °C 2.1: 86 percent / PBr3 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Ryan, William; Singer, Michael; Razdan, Raj K.; Compton, David R.; Martin, Billy R.
Life Sciences, 1995 , vol. 56, # 23/24 p. 2013 - 2020
反应条件
1: Et3N; diphenylphosphorazidate / benzene / 0.67 h 2: acetonitrile / 1 h / Heating View Scheme
参考文献
Song, Yu Min; Ha, Young Mi; Kim, Jin-Ah; Chung, Ki Wung; Uehara, Yohei; Lee, Kyung Jin; Chun, Pusoon; Byun, Youngjoo; Chung, Hae Young; Moon, Hyung Ryong
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7451 - 7455
反应条件
1,1'-carbonyldiimidazole in 1,2-dichloro-ethane
参考文献
Bauta, William E.; Lovett, Dennis P.; Cantrell Jr., William R.; Burke, Brian D.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5967 - 5973
反应条件
4: 28.8 g / fluoroboric acid, sodium nitrite / H2O 5: 7.6 g / warming, distillation View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
pyridine; thionyl chloride; silver(l) oxide 1. benzene, 1 h, reflux 2. ethyl ether, r.t., 1 h 3. reflux, 1 h; Yield given. Multistep reaction;
参考文献
Pang; Kozikowski
Journal of Organic Chemistry, 1991 , vol. 56, # 14 p. 4499 - 4508
反应条件
lithium aluminium tetrahydride in diethyl ether 16 h; Ambient temperature;
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
1: K2CO3 / acetone 2: LiAlH4 / diethyl ether 3: SOCl2 / diethyl ether View Scheme
参考文献
Kingston; Weiler
Canadian Journal of Chemistry, 1977 , vol. 55, # 5 p. 785 - 791
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Meier, Herbert; Dullweber, Uta
Tetrahedron Letters, 1996 , vol. 37, # 8 p. 1191 - 1194
