5-甲氧基-2-(苯基甲氧基)-苯丙醛合成路线 （共 7 条）
反应条件
pyridinium chlorochromate in dichloromethane T=0 - 20°C; 5 h; Inert atmosphereMolecular sieve;
参考文献
Dinda, Subal Kumar; Das, Sajal Kumar; Panda, Gautam
Synthesis, 2009 , # 11 art. no. Z01209SS, p. 1886 - 1896
反应条件
diisobutylaluminium hydride in toluene T=-78°C; 1 h; Inert atmosphere;
参考文献
Das, Sajal Kumar; Dinda, Subal Kumar; Panda, Gautam
European Journal of Organic Chemistry, 2009 , # 2 p. 204 - 207
反应条件
1.1: potassium carbonate / acetone / 6 h / Reflux 2.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 2.2: 6 h / Reflux 3.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1
反应条件
1.1: potassium carbonate / acetonitrile / 20 °C / Reflux 2.1: 16 h / 200 °C / Inert atmosphere 3.1: potassium carbonate / acetone / 6 h / Reflux 4.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 4.2: 6 h / Reflux 5.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1
反应条件
1.1: 16 h / 200 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 6 h / Reflux 3.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 3.2: 6 h / Reflux 4.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1
反应条件
1.1: potassium carbonate / acetone / 6 h / Reflux 2.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 2.2: 6 h / Reflux 3.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1
反应条件
1.1: 9-borabicyclo-[3.3.1]nonane / tetrahydrofuran / 4 h / 20 °C 1.2: 6 h / Reflux 2.1: pyridinium chlorochromate / dichloromethane / 5 h / 0 - 20 °C / Molecular sieve View Scheme
参考文献
UNIVERSITY OF NOTTINGHAM; BAKER, Jillian G.; FISCHER, Peter M.; FROMONT, Christophe; GARDINER, Sheila M.; HILL, Stephen J.; JADHAV, Gopal; KELLAM, Barrie; MISTRY, Shailesh; WOOLARD, Jeanette
Patent: WO2012/104659 A1, 2012 ;
WO 2012/104659 A1
