4,4'-二甲基-2,2'-联吡啶合成路线 （共 79 条）
反应条件
niobium bromide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionconstant current intensity 200 mA;
参考文献
Journal of Organic Chemistry, , vol. 67, # 6 p. 1838 - 1842
反应条件
palladium on activated charcoal
参考文献
Canadian Journal of Chemistry, , vol. 82, # 5 p. 595 - 607
反应条件
ammonium acetate; sodium hydroxide; acetic acid in tetrahydrofuran; toluene
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille-type cross-coupling; 48 h; Heating;
参考文献
Organic Letters, , vol. 2, # 21 p. 3373 - 3376
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
1.1: 48percent HBr; Br2 / 1.5 h / -20 °C 1.2: aq. NaNO2 / -20 - 15 °C 1.3: 85 percent / aq. NaOH / -10 - 20 °C 2.1: 67 percent / Pd(PPh3)4 / toluene / 48 h / Heating View Scheme
参考文献
Organic Letters, , vol. 2, # 21 p. 3373 - 3376
反应条件
hydrogenchloride in water 0.5 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 30, # 46 p. 6365 - 6368
