4,4'-二甲基-2,2'-联吡啶合成路线 （共 79 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
48 h; Ambient temperature;
参考文献
Ciana, Leopoldo Della; Hamachi, Itaru; Meyer, Thomas J.
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1731 - 1735
反应条件
1: 4,4'-dimethyl-2,2'-bipyridine With lithium diisopropyl amide in tetrahydrofuran; hexane
2 h; Inert atmosphere;
2: n-dodecyl iodide in tetrahydrofuran; hexane
T=0°C; 1.5 h; Inert atmosphere;
参考文献
Herbert, Matthew; Montilla, Francisco; Galindo, Agustin
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 338, # 1-2 p. 111 - 120
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
1.) 0 deg C, 1 h, 2.) 0 deg C, 30 min; 25 deg C, overnight;
参考文献
Griggs, Colin G.; Smith, David J. H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 12 p. 3041 - 3044
反应条件
1: 1.) LDA / 1.) THF, -78 deg C, 20 min; -78 deg C to -10 deg C, 25 min, 2.) -78 deg C, 10 s
2: 13 percent Chromat. / CsF / dimethylformamide / 24 h / 25 °C
View Scheme
参考文献
Fraser, Cassandra L.; Anastasi, Natia R.; Lamba, Jaydeep J. S.
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9314 - 9317
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
12 h; Ambient temperature;
参考文献
Torki, Farid M. el; Schmehl, Russell H.; Reed, Wayne F.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1989 , vol. 85, p. 349 - 362
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
12 h; Ambient temperature;
参考文献
Torki, Farid M. el; Schmehl, Russell H.; Reed, Wayne F.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1989 , vol. 85, p. 349 - 362
反应条件
lithium diisopropyl amide
1.) THF, 1.5 h; 2.) THF, 0 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Ellison, Dean K.; Iwamoto, Reynold T.
Tetrahedron Letters, 1983 , vol. 24, # 1 p. 31 - 32
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=100°C; 6 h;
参考文献
Berner; Klein; Nazeeruddin; De Angelis, Filippo; Castellani; Bugnon; Scopelliti; Zuppiroli; Graetzel
Journal of Materials Chemistry, 2006 , vol. 16, # 46 p. 4468 - 4474
反应条件
sodium sulfate; 3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 4 h;
参考文献
Ward, Robert S.; Branciard, Denis; Dignan, Rosemary A.; Pritchard, Martyn C.
Heterocycles, 2002 , vol. 56, # 1-2 p. 157 - 170
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Furue, Masaoki; Kuroda, Noritaka; Nozakura, Shun-ichi
Chemistry Letters, 1986 , p. 1209 - 1212
