3-甲基-2,4-壬烷二酮合成路线 （共 6 条）
反应条件
sodium chlorite; 4-hydroxy-TEMPO benzoate; sodium hydrogencarbonate; potassium bromide in dichloromethane T=5°C; 0.5 h;
参考文献
Yuasa, Yoshifumi; Kato, Yasushi
Organic Process Research and Development, 2002 , vol. 6, # 5 p. 628 - 631
反应条件
1: 2 percent aq. NaOH / 15 h / 20 - 25 °C 2: aq. sodium bicarbonate; 4-benzoyloxy-2,2,6,6-tetramethylpiperidine-N-oxide; sodium hypochlorate / potassium bromide / CH2Cl2 / 0.5 h / 5 °C View Scheme
参考文献
Kato; Yuasa
Journal of Agricultural and Food Chemistry, 2001 , vol. 49, # 8 p. 3864 - 3866
参考文献
Naef, Regula; Jaquier, Alaini; Velluz, Alain; Maurer, Bruno
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 24 p. 9201 - 9205
反应条件
oxygen; 5,15,10,20-tetraphenylporphyrin in hexane T=4°C; 24 h; exposure to high-intensity light; Further byproducts given. Title compound not separated from byproducts;
参考文献
Sigrist, Isabelle A.; Manzardo, Giuseppe G. G.; Amado, Renato
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 11 p. 3426 - 3428
反应条件
oxygen; 5,15,10,20-tetraphenylporphyrin in hexane T=4°C; 24 h; exposure to high-intensity light; Further byproducts given. Title compound not separated from byproducts;
参考文献
Sigrist, Isabelle A.; Manzardo, Giuseppe G. G.; Amado, Renato
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 11 p. 3426 - 3428
反应条件
oxygen; 5,15,10,20-tetraphenylporphyrin in hexane
T=4°C; 24 h; exposure to high-intensity light; Further byproducts given. Title compound not separated from byproducts;
参考文献
Sigrist, Isabelle A.; Manzardo, Giuseppe G. G.; Amado, Renato
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 11 p. 3426 - 3428
