反应条件
in tetrahydrofuran
(strict exclusion of air and moisture), Sn complex in THF cooled to -78°C under stirring, treated dropwise under vigorous stirring with C2HMgBr in THF, warmed to room temp., stirred for 12 h; concd.(vac.), suspnd.(hexane), filtered off, washed (hexane) 4 times, evapd., distilled (113°C, 7.5E-3 torr), crystd., elem. anal.;
参考文献
Wrackmeyer, Bernd; Thoma, Peter; Kempe, Rhett
European Journal of Inorganic Chemistry, 2009 , # 11 p. 1469 - 1476
