4,6-二甲氧基-2-甲磺酰基嘧啶合成路线 （共 13 条）
反应条件
Na2WO4·2H2O; tetrabutylammomium bromide; dihydrogen peroxide; acetic acid in water T=45 - 55°C;
参考文献
Xu, Defeng; Zhu, Zhiling; Xu, Hui; Wang, Ziqiao
Asian Journal of Chemistry, 2014 , vol. 26, # 1 p. 313 - 314
反应条件
potassium carbonate; sodium sulfite in tetrahydrofuran; methanol; water; ethyl acetate
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Substitution; 5 h;
参考文献
Tetrahedron, , vol. 56, # 27 p. 4739 - 4745
反应条件
1: POCl3 2: methanol 3: H2O2 in situ View Scheme
参考文献
Pest Management Science, , vol. 57, # 3 p. 205 - 224
反应条件
in ethanol 1.) ice bath, 2.) room temperature;
参考文献
Ishizumi; Kojima; Antoku
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 9 p. 2288 - 2300
反应条件
1: 2-hydroxybenzoic acid methyl ester With potassium carbonate T=20°C; 1 h; 2: 4,6-dimethoxy-2-methylsulfonyl-pyrimidine T=20°C; 18 h;
参考文献
Jin, Chuanfei; Liang, Yong-Ju; He, Hongwu; Fu, Liwu
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 10 p. 2096 - 2103
反应条件
potassium carbonate in tetrahydrofuran 8 h; Reflux;
参考文献
Chinese Journal of Chemistry, , vol. 28, # 10 p. 2020 - 2024
Heteroatom Chemistry, , vol. 21, # 3 p. 148 - 155
反应条件
potassium carbonate in butanone Substitution;
参考文献
Pesticide Science, , vol. 47, # 2 p. 115 - 124
反应条件
1: sodium hydrogen sulfide View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
反应条件
sodium hydrogensulfide
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
