1: 92 percent / triethylamine; bis(2-oxo-3-oxazolidinyl)phosphinic chloride / CH2Cl2 / 20.5 h / 20 °C
2: 90 percent / aqueous sodium hydroxide / dioxane / 19 h / 20 °C
View Scheme
参考文献
Harris, Paul W.R.; Brimble, Margaret A.; Muir, Victoria J.; Lai, Michelle Y.H.; Trotter, Nicholas S.; Callis, David J.
Tetrahedron, 2005 , vol. 61, # 42 p. 10018 - 10035
Clausen, Kim; Thorsen, Michael; Lawesson, Sven-Olov; Spatola, Arno F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 785 - 798