4-溴-2,6-二叔丁基苯酚合成路线 （共 45 条）
反应条件
perchloric acid; sodium perchlorate anodic oxidation;
参考文献
Chemische Berichte, , vol. 115, # 1 p. 288 - 308
反应条件
pyridine 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 46, # 22 p. 4454 - 4458
反应条件
dihydrogen peroxide; iodine in methanol; water T=35°C; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2006 - 2012
反应条件
1: 4-bromo-2,6-di-tert-butylphenol With sodium hydride in 1-methyl-pyrrolidin-2-one; mineral oil T=20°C; 0.5 h; Inert atmosphereCooling with ice; 2: N,N-dimethylthiocarbamoyl chloride in 1-methyl-pyrrolidin-2-one; mineral oil T=80°C; 4 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 2082 - 2093
反应条件
3-methoxy-phenol; copper; potassium carbonate in pyridine T=180°C; 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 493 - 497
反应条件
acetonitrile anodic oxidation;
参考文献
Chemische Berichte, , vol. 115, # 1 p. 288 - 308
反应条件
copper; potassium carbonate in pyridine T=180°C; 4 h; other temperature(100 deg C), other solvent (NN-diethylacetamide, 150 deg C; N-methylpyrrolidone, 185 deg C), analogous reaction with 2-methoxyphenol; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 493 - 497
反应条件
1: potassium; liquid NH3 2: H2SO4 View Scheme
参考文献
Hart; Cassis
Journal of the American Chemical Society, 1951 , vol. 73, p. 3179,3181
反应条件
N4S4 in toluene 1.5 h; Heating;
参考文献
Mataka, Shuntaro; Takahashi, Kazufumi; Shiwaku, Sohgo; Tashiro, Masashi
Journal of Chemical Research, Miniprint, 1985 , # 11 p. 3649 - 3665
反应条件
1.1: 97 percent / n-BuLi / tetrahydrofuran / -78 - 20 °C 2.1: t-BuLi; sulfur / tetrahydrofuran / -78 - -30 °C 2.2: tetrahydrofuran 3.1: 57 percent / Bu4NF / methanol / Heating View Scheme
参考文献
Bebbington, David; Monck, Nathaniel J. T.; Gaur, Suneel; Palmer, Alan M.; Benwell, Karen; Harvey, Victoria; Malcolm, Craig S.; Porter, Richard H. P.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 15 p. 2779 - 2782
