4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylazodicarboxylate in tetrahydrofuran
T=20°C; 11 h; Inert atmosphere;
参考文献
Singh, Santosh; Yadav, Lal Dhar S.
Tetrahedron Letters, 2012 , vol. 53, # 38 p. 5136 - 5140
反应条件
tetra-(n-butyl)ammonium iodide in benzene
T=20°C; 2 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
反应条件
InI in tetrahydrofuran
Michael addition; 3 h; Heating;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay
Canadian Journal of Chemistry, 2006 , vol. 84, # 5 p. 762 - 770
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.166667 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
pyridine in benzene
T=20°C; 27 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
参考文献
Lazar, J.; Vinkler, E.
Acta Chimica Academiae Scientiarum Hungaricae, 1980 , vol. 105, p. 171 - 174
反应条件
tetra-(n-butyl)ammonium iodide in benzene
T=20°C; 2 h;
参考文献
Levchenko, E. S.; Dubinina, T. N.; Budnik, L. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2158 - 2163
反应条件
CsOH in dimethyl sulfoxide
T=20°C; 20 h;
参考文献
Ouyang, Yue-Jun; Li, Yuan-Yuan; Li, Ning-Bo; Xu, Xin-Hua
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1103 - 1105
反应条件
1: 4,4'-dichlorodiphenyl disulfide With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran
T=20°C; Inert atmosphere;
2: acrylonitrile in tetrahydrofuran
T=20°C; 4.5 h; Inert atmosphere;
参考文献
Xu, Xiao Bo; Yin, Xian Hong; Zhu, Yu Yang; Xu, Xin Hua; Luo, Tao; Li, Yin Hui; Lu, Xiong; Shao, Ling Ling; Pan, Jian Gao; Yang, Rong Hua
Journal of Chemical Research, 2009 , # 12 p. 750 - 752
反应条件
fluorine in acetonitrile
T=-8 - 20°C; 24 h; Inert atmosphere;
参考文献
Pearhill Technologies LLC
Patent: US2010/22804 A1, 2010 ;
Location in patent: Page/Page column 7 ;
