4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
tert.-butylhydroperoxide
T=120°C; 18 h; Sealed tubeInert atmosphere;
参考文献
Du, Bingnan; Jin, Bo; Sun, Peipei
Organic Letters, 2014 , vol. 16, # 11 p. 3032 - 3035
反应条件
InI in tetrahydrofuran
Michael addition; 2.5 h; Heating;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay
Canadian Journal of Chemistry, 2006 , vol. 84, # 5 p. 762 - 770
反应条件
metal-assisted sulfenimine synthesis;
参考文献
Davis, Franklin A.; Lamendola, Joseph; Nadir, Upender; Kluger, Edward W.; Sedergran, Thomas C.; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2000 - 2005
反应条件
tert.-butylhydroperoxide; silver nitrate in water; acetonitrile
24 h; Reflux; chemoselective reaction;
参考文献
Das, Rima; Chakraborty, Debashis
Synthesis, 2011 , # 2 art. no. Z25110SS, p. 277 - 280
反应条件
sodium methylate in methanol
T=60 - 65°C; 3.5 h; Product distribution / selectivity;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2006/75139 A2, 2006 ;
Location in patent: Page/Page column 5 ;
WO 2006/075139 A2
反应条件
di-tert-butyl peroxide in neat (no solvent)
T=120°C; 12 h; Inert atmosphereSchlenk technique;
参考文献
Zeng, Jing-Wen; Liu, Yi-Chen; Hsieh, Ping-An; Huang, Yu-Ting; Yi, Chih-Lun; Badsara, Satpal Singh; Lee, Chin-Fa
Green Chemistry, 2014 , vol. 16, # 5 p. 2644 - 2652
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.5 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
1: 4,4'-dichlorodiphenyl disulfide With aluminium trichloride; zinc in water; acetonitrile
T=65°C; 1.5 h;
2: phenyl isocyanate in water; acetonitrile
T=65°C; 0.583333 h;
参考文献
Movassagh, Barahman; Zakinezhad, Yousef
Chemistry Letters, 2005 , vol. 34, # 10 p. 1330 - 1331
反应条件
potassium phosphate in dimethyl sulfoxide
T=40°C; 18 h;
参考文献
Movassagh, Barahman; Yousefi, Ali
Monatshefte fur Chemie, 2014 , vol. 145, # 7 p. 1173 - 1177
